(133)Vapor-Phase Method for the Preparation of Isocyanates. II. Synthesis of Higher Alkyl Isocyanates and Hexamethylenediisocyanate.

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A Convenient Method for the Synthesis of Sterically Hindered Aryl Isocyanates

Several methods have been reported for the syn­ thesis of isocyanates, most of them involving the use of phosgene: e.g. phosgene and primary amines [1] either in basic [2] or in acidic medium [1]; phosgene and diaryl urea [1]; phosgene and l-alkyl-3-arylsulphonyl urea [3]; or phosgene and sulfinyl amines [4], Isocyanates were further synthesized from olefins or alkyl halides by the use of isocy...

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ژورنال

عنوان ژورنال: The Journal of the Society of Chemical Industry, Japan

سال: 1953

ISSN: 0023-2734,2185-0860

DOI: 10.1246/nikkashi1898.56.289